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Pharmaceutical analysis 1st semester Handwritten notes pdf

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Click on the following download buttons below the names of the units to download Pharmaceutical Analysis both Handwritten and Standard Notes.

UNIT-1

(a) Analysis of pharmaceuticals- Definition, and scope

  1. Different methods of analysis
  2. Methods for expressing concentration
  3. Secondary & primary standards.
  4. Standardization & preparation of diverse normal & molar solutions - Oxalic acid the hydrochloric sodium acids, sodium thiosulphate, sulfuric acid, potassium permanganate, & ceric ammonium sulfate.

(b) Errors

  1. Causes of mistakes
  2. kinds of mistakes
  3. ways to minimize mistakes
  4. Accuracy
  5. precision
  6. significant figures

(c) Pharmacopoeia

  1. Impurities that are present in medicinal agents
  2. limit test

UNIT-2

(a) Acid-base Titration

  1. Theories about acid-base indicators
  2. Classification of acid-base titrations, & research in titrations of strong, weak, & very weak acids as well as bases
  3. Curves of neutralization

(b) Non-aqueous titration

  1. Solvents
  2. Acidimetry & Alkalimetry titration
  3. evaluation for Sodium benzoate as well as Ephedrine estimation of Sodium benzoate & Ephedrine

UNIT-3

(a) Titrations of precipitation

  1. Mohr's method
  2. The methodology used by Volhard
  3. Modified the method of Volhard
  4. Fajans method
  5. Estimation of sodium chloride

(b) Complexometric titration

  1. Type, indicators of metal ions as well as masking & demasking Reagents
  2. estimation of Magnesium sulfurate, & calcium gluconate.

(c) Gravimetry

  1. The principle & the steps involved with the analysis of gravity.
  2. Purity of the precipitate co-precipitation & post-precipitation
  3. Estimation of Barium Sulfate
  4. (d) Basic Methods, Principles, & application of diazotization the titration

UNIT-4

(a) Redox titrations

  1. Concepts of reduction & oxidation
  2. Different types of redox titrations (Principles as well as applications) Cerimetry & Iodimetry Iodometry, Bromatometry, Dichrometry Titration using potassium Iodate.

UNIT-5

(a) Methods of electrochemical analysis

Conductometry: Introduction, Conductivity cell Conductometric titrations & applications.
Potentiometry: Electrochemical cell design & operation of reference electrodes (Standard hydrogen electrode, silver chloride electrode, & the calomel electrode) along with the indicator electrodes (metal electrodes & glass electrodes) methods for determining the endpoint of potentiometric testing & its applications.
Polarography: Principle, Ilkovic equation, construction & operation of moving & dropping mercury electrodes, as well as the rotating electrode of platinum, application

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